Browsing by Subject "pitting corrosion"

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Access status: Open Access ,
Etching method to create random speckle pattern on semi-solid cast A356 aluminium for DIC in-situ strain measurement
(2017) Sergolle, Maëlle; Santos, Jorge; Kasvayee, Keivan Amiri; Jarfors, Anders Eric Wollmar
Aluminum semi-solid casting is constantly evolving, as it offers a combination of reduced shrinkage porosity and gas entrapment defects together with high productivity and an extended die-life. The relationship between the microstructure and stress-strain behavior is not well-understood due to its non-conventional microstructure. In-situ tensile testing, combined with optical microscope and Digital Image Correlation (DIC), has been used for local strain distribution measuements in cast irons. The critical capability was an etching technique to generate a micro-scale random speckle pattern with a sufficiently high speckle density to enable the sufficient spatial resolution of displacement and strain. The current paper focuses on the development of a pit etching procedure for the semi-solid cast A356 aluminum alloy to study local strain accommodation on the microstructure during tensile loading. The critical challenge of this procedure was the generation of homogeneously distributed pits on both the primary aluminum and eutectic regions. Therefore, a heated solution used for wet-etch aluminum in microfabrication was modified as well as a process adapted to generate pits with suitable characteristics. In-situ tensile tests were performed attached to an optical microscope to record the microstructure and displacements during loading. DIC software was used for analysis. The procedure was validated through a comparison between the resulting Young´s moduls using standard tensile testing and the DIC process on the speckle pattern generated. A good fit between the two methods for Young´s modulus was found. The spatial resolution obtained was, however, not sufficient to fully resolve the strain gradients in the microstructure, but it did reveal large strain variations in the microstructure.
Access status: Open Access ,
Influence of corrosion on mechanical properties and microstructure of 3xxx, 5xxx, and 6xxx series aluminum alloys
(Wydawnictwa AGH, 2017) Ziobro, Grzegorz; Richert, Maria Wiesława; Wiewióra, Marcel
Growing demands imposed on passenger car producers concerning the reduction of exhaust emission to the environment are forcing a search for new materials and design solutions. One of the most-important factors that can reduce this emission is the low mass of a vehicle, leading to a decrease in its average fuel consumption. A reduction in weight can be obtained by the use of aluminum elements instead of steel, e.g., in air conditioning pipes, decreasing the specific weight of the construction by nearly three times. In the present study, the influence of the SWAAT corrosion test on A/C piping made from 3xxx, 5xxx, and 6xxx series aluminum alloys was investigated. The study focused on changes in the mechanical properties of samples before and after a SWAAT test determined by a tensile test and Vickers hardness measurements. Additionally, microstructure examinations were performed with the use of optical and scanning microscopy. Corrosion products on the surface of pipes were identified by Energy Dispersive X-ray Spectroscopy. Pipes made from the EN AW 6063 alloy revealed an almost 50% decrease in its strength properties after the tests. The largest decline in plastic properties was observed in pipes made from the EN AW 6060 alloy.
Access status: Open Access ,
The effect of rapid cooling on the corrosion resistance of as-cast aluminium alloy 5052
(AGH University of Science and Technology Press, 2017) Szklarz, Zbigniew; Krawiec, Halina; Rogal, Łukasz
The effect of rapid cooling by the vacuum suction casting method (VSC) on the microstructure and electrochemical response of the as-cast 5052 aluminium alloy is presented. The VSC method allowed us to obtain massive samples with a very high cooling rate (10$^{2}$ - 10$^{3}$)°C/s. The microstructure of the quick-cooled sample (QC) has been significantly changed. Finer grains and more-homogeneous intermetallic phase distribution has been observed. Corrosion potential (OCP) and polarization measurements (LSV) revealed a higher activity of the QC alloy than ingot (IN), which leads to a denser and thicker corrosion-product formation on the surface. Electrochemical Impedance Spectroscopy (EIS) indicates higher resistance values, which suggests a greater thickness of the corrosion products.